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Manufacturing Diamond Under Very High Pressure

Pure or doped diamond is crystallized from molten carbon and in solid state. A process for manufacturing bulk diamond has been made practical by the invention of the High Pressure and Temperature Apparatus capable of applying the combination of very high temperature and high pressure needed to melt carbon in a sufficiently large volume. The rate of growth achievable in this process is about ten times the rate achievable in older processes. Depending on the starting material and temperature-and-pressure schedule, this process can be made to yield diamond in any of a variety of scientifically and industrially useful forms, including monocrystalline, polycrystalline, pure, doped, and diamond composite. (Doping makes it possible to impart desired electrical and optical properties, including semiconductivity and color.) The process can also be used to make cubic boron nitride.

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A Method of Assembling Compact Coherent Fiber-Optic Bundles

The method is based on hexagonal close packing. A method of assembling coherent fiber-optic bundles in which all the fibers are packed together as closely as possible is undergoing development. The method is based straightforwardly on the established concept of hexagonal close packing; hence, the development efforts are focused on fixtures and techniques for practical implementation of hexagonal close packing of parallel optical fibers.

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Fabrication of Submillimeter Axisymmetric Optical Components

Surfaces of components can be arbitrarily shaped to optimize spectral responses. It is now possible to fashion transparent crystalline materials into axisymmetric optical components having diameters ranging from hundreds down to tens of micrometers, whereas previously, the smallest attainable diameter was 500 m. A major step in the fabrication process that makes this possible can be characterized as diamond turning or computer numerically controlled machining on an ultrahigh-precision lathe. This process affords the flexibility to make arbitrary axisymmetric shapes that have various degrees of complexity: examples include a flat disk or a torus supported by a cylinder (see figure), or multiple closely axially spaced disks or tori supported by a cylinder. Such optical components are intended mainly for use as whispering-gallery- mode optical resonators in diverse actual and potential applications, including wavelength filtering, modulation, photonic generation and detection of microwaves, and research in quantum electrodynamics and quantum optics.

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Process for Polishing Bare Aluminum to High Optical Quality

India-ink polishing following single-point diamond turning yields superior aluminum optics. A process for making precise, high-quality curved or flat mirror surfaces on bare aluminum substrates has been devised. The process consists of (1) diamond turning to establish the desired surface figure, followed by (2) a polishing subprocess that is mostly conventional except for the composition of the polishing compound. This process can maintain a surface figure accurate to within a peak-to-valley error of as little as 1/8 wavelength (at a wavelength of 6,328 Å) and can produce a finish characterized by a root-mean-square roughness of

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Radiation-Shielding Polymer/Soil Composites

Radiation shields could be fabricated in situ at relatively low cost. It has been proposed to fabricate polymer/soil composites primarily from extraterrestrial resources, using relatively lowenergy processes, with the original intended application being that habitat structures constructed from such composites would have sufficient structural integrity and also provide adequate radiation shielding for humans and sensitive electronic equipment against the radiation environment on the Moon and Mars. The proposal is a response to the fact that it would be much less expensive to fabricate such structures in situ as opposed to transporting them from Earth.

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Film/Adhesive Processing Module for Fiber-Placement Processing of Composites

Films, foils, or adhesives may be interleaved while fiber-placing composite material structures. An automated apparatus has been designed and constructed that enables the automated lay-up of composite structures incorporating films, foils, and adhesives during the automated fiberplacement process. This apparatus, denoted a film module, could be used to deposit materials in film or thin sheet form either simultaneously when laying down the fiber composite article or in an independent step. Examples of materials that may be processed with this device include structural core and joining adhesives, permeation barrier films/foils, surfacing films, lightning-strike materials and IVHM (Integral Vehicle Health Monitoring) arrays. The use of this technology will reduce composite fabrication time and will allow for new concepts/ designs to be considered for fiber-placed composite structures.

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Automated Solvent Seaming of Large Polyimide Membranes

Success depends on precise control of all relevant process details. A solvent-based welding process enables the joining of precise, cast polyimide membranes at their edges to form larger precise membranes. The process creates a homogeneous, optical - quality seam between abutting membranes, with no overlap and with only a very localized area of figure disturbance. The seam retains 90 percent of the strength of the parent material. The process was developed for original use in the fabrication of wide - aperture membrane optics, with areal densities densities of less than 1 kg/m2, for lightweight telescopes, solar concentrators, antennas, and the like to be deployed in outer space. The process is just as well applicable to the fabrication of large precise polyimide membranes for flat or inflatable solar concentrators and antenna reflectors for terrestrial applications.

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