Physical Sciences

Ultrahigh-Vacuum Arc-Jet Source of Nitrogen for Epitaxy

Electron-excitation and translational energies can be selected. An arc-jet source of chemically active nitrogen atoms has been developed for use in molecular-beam epitaxy (MBE) to grow such III-V semiconductors as nitrides of gallium, aluminum, and indium. This apparatus utilizes a confined arc to thermally excite N2 and to dissociate N2 into N atoms. This apparatus is compatible with other, ultrahigh-vacuum MBE equipment commonly used in growing such materials.

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Lightweight Mirrors for Orbiting Earth-Observing Instruments

A report discusses selected aspects of a continuing program to develop thermally stable, lightweight mirrors for planned Earth-observing spaceborne instruments. These mirrors are required to retain precise concave or convex surface figures required for diffraction-limited optical performance, even in the presence of transient, asymmetric thermal loads, which include solar heating and radiational cooling. In the first phase of the program, preliminary analyses were performed to select one of three types of mirror structures: one made of SiC, one made of Be, and a hybrid comprising a lightweight composite-material substructure supporting a glass face sheet that would be a substrate for the required precise optical surface. The hybrid structure was selected for further development because it would offer a combination of high stiffness and low mass and because, relative to the Be and SiC structures, (1) the coefficients of thermal expansion of its constituent materials and the resulting wavefront error would be smaller, and (2) it could be fabricated at lower cost. A prototype hybrid structure with an aperture diameter of 0.3 m was fabricated. Planned efforts in the next phase of the program include optical polishing of the glass face sheet and testing.

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Electrostatic/Electrodynamic Nanoparticle-Capture Vessel

Particles could be sampled under remote or automatic control in harsh environments. A proposed simple, portable, robust apparatus, capable of automated operation, has been proposed for collecting samples of selected biological or chemical species in harsh environments. The sampled species could range in size from molecules to nanoparticles (that is, particles with dimensions of the order of nanometers). The apparatus would select a biological or chemical species of interest for sampling by utilizing a combination of (1) electrostatic or electrodynamic fields and (2) a sieve containing holes of predetermined size.

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Radiometer for Measuring Cirrus-Cloud Ice and Water Vapor

Accurate measurements would contribute to understanding of weather and climate. An airborne submillimeter-wavelength radiometer, expected to be built and tested in the near future, is designed primarily to yield measurement data that can be processed to quantify the ice contents and mean sizes (and, to some extent, the shapes) of ice crystals in cirrus clouds that range from optically thin to opaque. Secondarily, this radiometer is also designed to enable the characterization of watervapor profiles in the presence of optically thick clouds. The ice and water-vapor data are needed to improve understanding of processes that affect weather and climate.

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System For Measuring Osmotic Transport Properties of a Membrane

Membrane-testing operations are performed automatically. The membrane test cell (MTC) is an automated laboratory apparatus that applies a known osmotic potential across a membrane and measures the kinetics of the resulting transport of solvents across the membrane as a function of time. Data acquired by use of the MTC should prove especially helpful in designing industrial processes that rely on membrane separation techniques. Examples of such processes include desalination, recovery of designated chemicals from process streams, and some recycling operations.

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Vacuum Leak Detection Using Piezoelectric Film

A technique for detecting a small leak of gas into a vacuum involves the use of a diaphragm made of a thin film of poly (vinylidene fluoride) [PVDF]. To exploit the piezoelectricity of PVDF for this purpose, both sides of the film are coated with thin, electrically conductive layers that serve as electrodes. Wires connect the electrodes to the input terminals of a buffer amplifier and associated circuitry that measures the voltage induced between the electrodes by the piezoelectric effect in the film. In operation, the diaphragm is moved around in the vacuum in the vicinity of, and facing toward, a suspected leak. When the diaphragm crosses the stream of leaking gas, the pressure of the gas impinging on the diaphragm bends the diaphragm, thereby inducing a voltage. In an experiment, a prototype sensor based on this concept generated a signal of about 60 mV from air leaking into a vacuum through an orifice 10 μm wide at a rate of 0.017 standard cm3/s. The noise floor of the sensor was found to be about 5 mV. It was concluded that even this initial unoptimized sensor should be able to detect leaks somewhat smaller than 0.01 standard cm3/s.

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Quasi-Decoupling of Shvab-Zel’dovich Variables

A paper presents some novel conclusions concerning the Shvab-Zel’dovich (SZ) vari- ables, which are linear combinations of dep- endent variables in mathematical models of multicomponent, chemically reacting flows. The SZ variables represent scalar quantities that are conserved, that is, are not affected by chem- istry. The role of SZ variables is to decouple the conservation equations and make it simpler to solve them. However, SZ variables that entirely decouple the system of equations are generally defined only under the restrictive assumption that all Lewis numbers are unity (ALeU). Each Lewis number represents the ratio of a single species mass-diffusion characteristic time to the thermal conduction characteristic time. The present paper discusses the foregoing issues and further presents a mathematical analysis addressing the question of whether the ALeU assumption is a necessary condition for such decoupling. The conclusion reached in the analysis is that the ALeU assumption is sufficient but not necessary and that quasi-decoupling (that is partial decoupling) may be performed in the absence of thermal diffusion. When thermal diffusion is present, quasi-decoupling may still be performed subject to a controllable error.

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