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A Continuous-Flow, Microfluidic, Microwave-Assisted Chemical Reactor

The reactor uses a directed 60-GHz source, which may require far less power to observe the same reactivity profiles. NASA’s Jet Propulsion Laboratory, Pasadena, California In industrial synthetic chemistry laboratories, reactions are generally carried out using batch-mode methodologies, stepwise reactions, and purifications to generate a final product. Each step has an associated yield of both the reaction itself and of the final purification that is largely dependent on the procedure being used, and the scientist carrying out the procedure. Continuous-flow reactors are one way of streamlining the process. Furthermore, microwave-enhanced, or microwave-assisted, chemistry has been demonstrated to aid in many of these areas; however, scaling has been a traditional problem with this technique.

Posted in: Articles, Briefs, TSP

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High-Resolution Data Acquisition System Enables Reliable Engine Parameter Measurements

Obtaining accurate measurements is critical for improving vehicle component performance and overall system reliability. HBM, Inc., Marlborough, Massachusetts Data acquisition plays a critical role in improving vehicle component performance and overall system reliability. Measuring engine parameters, including engine cranking speed and the mechanical condition of the engine, requires high-resolution data acquisition equipment.

Posted in: Articles, Briefs, Data Acquisition, Measuring Instruments

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Guarded Flat Plate Insulation Test Cryostat

Features include high testing rate and high data quality. John F. Kennedy Space Center, Florida The guarded flat plate insulation test cryostat (Cryostat-500) is a boil-off calorimeter comprising a flat-bottom test apparatus for measuring the absolute thermal performance of an insulation test article. Typical dimensions allow accepting test specimens 200 mm in diameter by up to 30 mm thick. The test chamber is guarded by a second cryogen chamber to prevent parasitic heat loads. System insulation materials provide additional thermal stability for testing over a wide range of environmental conditions. The cold-mass assembly can be configured for rigid or soft materials, with or without compressive loads.

Posted in: Articles, Briefs, Data Acquisition

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High-Performance Polyimide Powder Coatings

Applications include bridges, pipes, machinery, exposed metal parts and structures, and automobile components. John F. Kennedy Space Center, Florida Powder coatings are used throughout industry to paint a myriad of metallic objects. This method of coating has gained popularity because of its conservation of materials and elimination of volatile organic compounds (VOCs). Resins used in powder coatings are traditionally chosen from those that have low melting points (polyesters, acrylics, urethanes, epoxies, etc.). These resins are used because they can melt and flow into a smooth coating before curing to a durable surface. High-performance resins such as Teflon, nylon, and polyimide have not found use in powder coatings because of their high melting points.

Posted in: Articles, Briefs, Coatings & Adhesives

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Selective Functionalization of Carbon Nanotubes

Lyndon B. Johnson Space Center, Houston, Texas This invention is a process by which carbon nanotubes can be chemically functionalized according to their precise electronic structure. The process involves an exploitation of charge transfer stability at the nanotube sidewall to direct selective reaction of certain electronic structures over others. This process forms the basis for manipulating and separating carbon nanotubes by their electronic structure by chemical means.

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Predictive Modeling of Corrosion Efficiencies and Toxicities

An analytical approach using a combination of descriptors successfully predicts the performance of a wide range of organic corrosion inhibitors. John F. Kennedy Space Center, Florida Atmospheric corrosion is significantly accelerated by the presence of heat, humidity, corrosive salts, and sunlight. At Kennedy Space Center (KSC), all of these accelerants are present, producing an extremely corrosive environment. Toxicity and environmental impacts of some inorganic corrosion inhibitors have severely limited the use of some of the most effective corrosion inhibitors. Unfortunately, robust, low-toxicity, high-performance organic corrosion inhibitors for coatings are not yet at a stage to replace the most effective inorganic inhibitors.

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Improving Foreign Object Damage Performance for 2D Woven Ceramic Matrix Composites

A model simulates high-speed impact response of ceramic matrix composites. John H. Glenn Research Center, Cleveland, Ohio As the power density of advanced engines increases, the need for new materials that are capable of high operating temperatures, such as ceramic matrix composites (CMCs), is critical for turbine hot-section static and rotating components. Such advanced materials can significantly increase engine operating temperatures relative to those with conventional superalloy metallic blades. They also show the potential to enable longer life, growth margin, reduced emissions, reduced weight, and increased performance when compared with superalloy blade materials.

Posted in: Articles, Briefs, TSP, Composites

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